FTIR(傅里叶变换红外光谱仪)是一种红外光谱仪测量方法。
用红外光照射样品(固体、液体或气体),然后使用干涉仪干涉透射光或反射光,并通过傅里叶变换信号强度来获取光谱信息。
由于可以根据获得的光谱信息对物质进行定性、定量和识别,因此使用 FTIR 的分析仪和分光光度计被广泛应用于医疗、化学、环境和材料分析等各个领域。
根据所处理的红外光的波长范围,其有时被区分为 FT-NIR(近红外光)或 FT-IR(中红外光)。
波长 (μm) | FT-NIR | FT-IR | |||
---|---|---|---|---|---|
1 | 2 | 5 | 10 | 15 | |
光谱仪 |
(1.1 ~ 2.5 μm) |
||||
红外探测器 |
(1 ~ 2.5 μm) |
||||
(1 ~ 3.8 μm) |
|||||
(1 ~ 5.5 μm) |
|||||
(1 ~ 11. μm) |
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(1 ~ 14.5 μm) |
FTIR 引擎(FT-NIR 光谱仪)是一种紧凑型傅里叶变换红外光谱仪模块,将迈克尔逊光干涉仪和控制电路组合在一个手掌大小的外壳中。我们将独特的 MEMS 技术和安装技术应用于光干涉仪,在保留傅里叶变换型特点的同时,使 FTIR 引擎的外形更加紧凑。
为了消除由小型化引起的入射光量的降低,我们使用滨松的原创 MEMS 技术开发了一种可动反射镜。该反射镜在光干涉仪内构成执行器,然后借此进行改进,以便高效利用反射光。此外,我们将可动反射镜和固定反射镜集成为 MEMS 芯片,从而使其结构紧凑,并将反射镜之间的相对角度误差减小至约 1/100。通过优化 MEMS 执行器的结构和驱动方法,消除运行期间的模糊问题,我们抑制了光干涉仪内部的红外光扩散,并减少了损耗。如此一来,我们实现了堪比传统固定式设备的检测性能。
当被测量的光(入射光)被分束器分割,被可动反射镜和固定反射镜反射,然后再次结合时,就会发生光干涉。根据可动反射镜的位置变化的干涉光强度由光电检测器(InGaAs PIN 光电二极管)检测,然后对信号进行算术处理(傅里叶变换)以获得光谱。通过使用光电检测器(硅 PIN 光电二极管)和半导体激光器 (VCSEL) 测量干涉仪内部可动反射镜的位置,可以获得具有高波长再现性的光谱。
1.1 μm 至 2.5 μm 的近红外区域在各个领域用于红外光谱分析,因为许多材料在此区域具有独特的吸收光谱。
使用 FTIR 引擎的红外光谱分析有两种类型:反射测量和透射测量。
FTIR 中使用的许多中红外光电检测器都含有 RoHS 指令限制的物质,因此需要开发替代产品。
作为可检测波长达 14.5 μm 的化合物光电半导体设备,我们成功量产了全球第一款不使用 RoHS 指令限制物质(汞和镉)的 II 型超晶格红外探测器。
还提供带有前置放大器的模块,只需连接直流电源即可操作。
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